Making Liquid Oxygen: Far From Easy But Worth The Effort

Normally, videos over at The Signal Path channel on YouTube have a certain vibe, namely teardowns and deep dives into high-end test equipment for the microwave realm. And while we always love to see that kind of content, this hop into the world of cryogenics and liquid oxygen production shows that [Shahriar] has other interests, too.

Of course, to make liquid oxygen, one must first have oxygen. While it would be easy enough to get a tank of the stuff from a gas supplier, where’s the fun in that? So [Shahriar] started his quest with a cheap-ish off-the-shelf oxygen concentrator, one that uses the pressure-swing adsorption cycle we saw used to great effect with DIY O2 concentrators in the early days of the pandemic. Although analysis of the machine’s output revealed it wasn’t quite as capable as advertised, it still put out enough reasonably pure oxygen for the job at hand.

The next step in making liquid oxygen is cooling it, and for that job [Shahriar] turned to the cryocooler from a superconducting RF filter, a toy we’re keen to see more about in the future. For now, he was able to harvest the Stirling-cycle cryocooler and rig it up in a test stand with ample forced-air cooling for the heat rejection end and a manifold to supply a constant flow of oxygen from the concentrator. Strategically placed diodes were used to monitor the temperature at the cold end, a technique we can’t recall seeing before. Once powered up, the cryocooler got down to the 77 Kelvin range quite quickly, and within an hour, [Shahriar] had at least a hundred milliliters of lovely pale blue fluid that passed all the usual tests.

While we’ve seen a few attempts to make liquid nitrogen before, this might be the first time we’ve seen anyone make liquid oxygen. Hats off to [Shahriar] for the effort.

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Open-Source Oxygen Hack Chat

Join us on Wednesday, May 5 at noon Pacific for the Open-Source Oxygen Hack Chat with Maher Daoudi and the OxiKit Team!

In such tumultuous times, it may be hard to remember last week, let alone last year. But if you dig back a bit, you may recall what a panic the world was in at this point in 2020 about the ventilator crisis. With COVID-19 cases on the rise and the potential for great numbers of patients needing intensive care, everyone and their brother was hacking together makeshift ventilators, in the well-intentioned belief that their inventions would help relieve the coming shortage of these lifesaving medical mechanical miracles.

As it came to pass, though, more COVID-19 patients have benefited from high-flow oxygen therapy than from mechanical ventilation. That’s great news in places where medical oxygen is cheap and easily available, but that’s always the case. We’ve seen recent reports of hospitals in India running out of oxygen, and even rural and remote areas of the developed world can find themselves caught without enough of the vital gas.

To meet the world’s increasing demand for high-flow oxygen therapy, the team at OxiKit has developed an open-source oxygen concentrator that can be built for far less than what commercial concentrators cost. By filtering the nitrogen out of the air, the concentrator provides oxygen at 90% or higher purity, at a flow of up to 25 liters per minute.

Oxikit founder Maher Daoudi and some of the technical team will join us for this Hack Chat to discuss the details of making oxygen concentrators. We’ll learn about how they work, what the design process for their current concentrator was like, and how they got past the obstacles and delivered on the promise of high-flow oxygen for the masses.

join-hack-chatOur Hack Chats are live community events in the Hackaday.io Hack Chat group messaging. This week we’ll be sitting down on Wednesday, May 5 at 12:00 PM Pacific time. If time zones have you tied up, we have a handy time zone converter.

Click that speech bubble to the right, and you’ll be taken directly to the Hack Chat group on Hackaday.io. You don’t have to wait until Wednesday; join whenever you want and you can see what the community is talking about.
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A Simple But Effective High-Flow Oxygen Concentrator From Hardware Store Parts

To say that a lot has happened in the year since the COVID-19 pandemic started is an understatement of epic proportions, so much so that it may be hard to remember how the hardware hacking community responded during those early days, with mass-produced PPE, homebrew ventilators and the like. But we don’t recall seeing too many attempts to build something like this DIY oxygen concentrator during that initial build-out phase.

Given the simplicity and efficacy of the design, dubbed OxiKit, it seems strange that we didn’t see more of these devices. OxiKit uses zeolite, a porous mineral that can be used as a molecular sieve. The tiny beads are packed into columns made from hardware store PVC pipes and fittings and connected to an oil-less air compressor through some solenoid-controlled pneumatic valves. After being cooled in a coil of copper pipe, the compressed air is forced through one zeolite column, which preferentially retains the nitrogen while letting the oxygen pass through. The oxygen stream is split, with part going into a buffer tank and part going into the outlet of the second zeolite column, where it forces the adsorbed nitrogen to be released. An Arduino controls the valves that alternate the gas flow back and forth, resulting in 15 liters per minute of 96% pure oxygen.

OxiKit isn’t optimized as a commercial oxygen concentrator is, so it’s not particularly quiet. But it’s a heck of a lot cheaper than a commercial unit, and an easy build for most hackers. OxiKit’s designs are all open source, but they do sell kits and some of the harder-to-source parts and supplies, like the zeolite. We’d be tempted to build something like this just because the technology is so neat; having a source of high-flow oxygen available isn’t a bad idea, either.