Spectrometry is a well-known technique or, more correctly, a set of techniques. We usually think of it as the analysis of light to determine what chemicals are producing it. For example, you can tell what elements are in a star or an incandescent based on the spectrum of light they emit. But you can also do spectroscopy with other ranges of electromagnetic radiation. [Applied Science] shows how to make an RF spectroscope. You can see the video below.
An oscilloscope-resident function generator creates a signal that he feeds to an amplifier because you need a fair amount of power going out. However, you also need to sense a very tiny amount of power coming back, and that requires a special circuit that will block high-power signals while passing low-level signals.