“You can never be too rich or too thin,” the saying goes, and when it comes to coatings, it’s true that thinner is often better. The way to truly thin coatings, ones that are sometimes only a few atoms thick, is physical vapor deposition, or PVD, a technique where a substance is transformed into a vapor and condensed onto a substrate, sometimes using a magnetron to create a plasma.
It sounds complicated, but with a few reasonable tools and a healthy respect for high voltages, a DIY magnetron for plasma sputtering can get you started. To be fair, [Justin Atkin] worked on his setup for years, hampered initially by having to settle for found parts and general scrap for his builds. As with many things, access to a lathe and the skills to use it proved to be enabling, allowing him to make custom parts like the feedthrough for the vacuum chamber as well as a liquid-cooled base, which prevents heat from ruining the magnets that concentrate the plasma onto the target metal. Using a high-voltage DC supply made from old microwave parts, [Justin] has been able to sputter copper films onto glass slides, with limited success using other metals. He also accidentally created a couple of dichroic mirrors by sputtering with copper oxides rather than pure copper. The video below has some beautiful shots of the ghostly green and purple glow.
A rig such as this opens up a lot of possibilities, from optics to DIY semiconductors. It may not be quite as elaborate as some PVD setups we’ve seen, but we’re still pretty impressed.
Continue reading “Vacuum Sputtering With A Homemade Magnetron”
If you are an astronomer with an optical reflecting telescope, the quality of your mirror is one of your most significant concerns. Large observatories will therefore often have on-site vapour deposition plants to revitalise their reflectors by depositing a fresh layer of aluminium upon them. You might think that such a device would be the preserve only of such well-funded sites, but perhaps [Michael Koch]’s work will prove you wrong. He’s created his own vapour deposition system (Google Translate link of the German original) from scratch, and while it might be smaller than the institutional equivalents it is no less effective in its task.
At the heart of it is a stainless steel vacuum vessel with a two stage vacuum pump system to evacuate it. The mirror to be silvered is suspended in the vessel, and a piece of aluminium is suspended over a coil of tungsten wire that his electrically heated to melt it. The molten aluminium is described as “wetting” the tungsten wire in the same manner as we’ll be used to solder working on copper, but in the vacuum it vaporizes and deposits itself upon the mirror. Such a simple description glosses over the impressive work that went into it.
This is a long-running project that isn’t entirely new, but very much worth a look if only for its introduction to this fascinating field. If you are new to vacuum work, how about looking at a Superconference presentation introducing vacuum technology?
Thanks [Paul Bauer] for the tip.