chemistry hacks

604 Articles

Diamond Batteries That Last For Millennia

November 29, 2016 by 72 Comments

Like many industrialized countries, in the period after the Second World War the United Kingdom made significant investments in the field of nuclear reactors. British taxpayers paid for reactors for research, the military, and for nuclear power.

Many decades later that early crop of reactors has now largely been decommissioned. Power too cheap to meter turned into multi-billion pound bills for safely coping with the challenges posed by many different types of radioactive waste generated by the dismantling of a nuclear reactor, and as the nuclear industry has made that journey it in turn has spawned a host of research projects based on the products of the decommissioning work.

One such project has been presented by a team at Bristol University; their work is on the property of diamonds in generating a small electrical current when exposed to radioactive emissions. Unfortunately their press release and video does not explain the mechanism involved and our Google-fu has failed to deliver, but if we were to hazard a guess we’d ask them questions about whether the radioactivity changes the work function required to release electrons from the diamond, allowing the electricity to be harvested through a contact potential difference. Perhaps our physicist readers can enlighten us in the comments.

So far their prototype uses a nickel-63 source, but they hope to instead take carbon-14 from the huge number of stockpiled graphite blocks from old reactors, and use it to create radioactive diamonds that require no external source. Since the output of the resulting cells will be in proportion to their radioactivity their life will be in the same order of their radioactive half-life. 5730 years for half-capacity in the case of carbon-14.

Of course, it is likely that the yield of electricity will not be high, with tiny voltages and currents this may not represent a free energy miracle. But it will be of considerable interest to the designers of ultra-low-maintenance long-life electronics for science, the space industry, and medical implants.

We’ve put their video below the break. It’s a straightforward explanation of the project, though sadly since it’s aimed at the general public it’s a little short on some of the technical details. Still, it’s one to watch.

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Scrap Bin Mods Move Science Forward

November 20, 2016 by 12 Comments

A first-time visitor to any bio or chem lab will have many wonders to behold, but few as captivating as the magnetic stirrer. A motor turns a magnet which in turn spins a Teflon-coated stir bar inside the beaker that sits on top. It’s brilliantly simple and so incredibly useful that it leaves one wondering why they’re not included as standard equipment in every kitchen range.

But as ubiquitous as magnetic stirrers are in the lab, they generally come in largish packages. [BantamBasher135] needed a much smaller stir plate to fit inside a spectrophotometer. With zero budget, he retrofitted the instrument with an e-waste, Arduino-controlled magnetic stirrer.

The footprint available for the modification was exceedingly small — a 1 cm square cuvette with a flea-sized micro stir bar. His first stab at the micro-stirrer used a tiny 5-volt laptop fan with the blades cut off and a magnet glued to the hub, but that proved problematic. Later improvements included beefing up the voltage feeding the fan and coming up with a non-standard PWM scheme to turn the motor slow enough to prevent decoupling the stir bar from the magnets.

[BantamBasher135] admits that it’s an ugly solution, but one does what one can to get the science done. While this is a bit specialized, we’ve featured plenty of DIY lab instruments here before. You can make your own peristaltic pump or even a spectrophotometer — with or without the stirrer.

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Open Microfluidics Instrumentation Playset

November 17, 2016 by 17 Comments

Micro-what? Microfluidics! It’s the field of dealing with tiny, tiny bits of fluids, and there are some very interesting applications in engineering, biology, and chemistry. [Martin Fischlechner], [Jonathan West], and [Klaus-Peter Zauner] are academic scientists who were working on microfluidics and made their own apparatus, initially because money was tight. Now they’ve stuck to the DIY approach because they can get custom machinery that simply doesn’t exist.

In addition to their collaboration, and to spread the ideas to other labs, they formed DropletKitchen to help advance the state of the art. And you, budding DIY biohacker, can reap the rewards.

In particular, the group is focused on droplet microfluidics. Keeping a biological or chemical reaction confined to its own tiny droplet is like running it inside its own test-tube, but because of the high rate at which the droplets can be pumped out, literally millions of these test-tubes are available. Want to grow hundreds of thousands of single cells, each in their own environment? Done.

The DropletKitchen kit includes an accurate pump system, along with high-speed camera and flash setups to verify that everything’s working as it should. Everything is open-source, and a lot of it is 3D-printable and written in OpenSCAD so that it’s even easy to modify to fit your exact needs. You just need to bring the science.

This is a professional-grade open source project, and we’re excited to see it when academics take a turn toward the open. Bringing cutting edge processing technologies within reach of the biohacker community is a huge multiplier. We can’t wait to see what comes out of this.

Make Water Bridges With High Voltages

November 15, 2016 by 42 Comments

It’s generally a bad idea to mix high voltage electricity and water, but interesting things happen if you do. This video from [RWGResearch] shows one of them: water bridging. If you have two water sources (such as two beakers full of very highly distilled water) with a high voltage between them, the voltage can create a gravity defying bridge that flows between them.

The experiment starts with the pouring spouts from two beakers nearly touching each other. Water fills the beakers right up to the spout, but it’s the application of electricity that pulls the bridge between the positive and negative beakers. With care, this technique can create a bridge of up to 2cm (about 0.8 inches). [RWGResearch] shows that he is able to create a bridge of about a centimeter with a 5KV voltage, but which only carries a few milliamps.

What forces are at play here isn’t exactly clear, but one recent paper speculates that it’s down to a combination of the dielectric force caused by the differing charges of parts of water molecules and the surface tension of the water. Whatever it is, it is fascinating and makes for a neat trick.

Want to make your own contribution to the scientific body of knowledge? Prove or disprove the speculation mentioned in the Wikipeadia article: is this possible because of an H3O2 lattice formed by the high voltage? How would you formulate a test for this?

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Transparent Rocket Engine

November 12, 2016 by 45 Comments

Rocket engines are undeniably cool. Experiencing the roar, seeing the fire, and watching the rocket blast off into the sky… what else can you ask for? Well, for [NightHawkInLight], a transparent rocket body is the answer.

Based on previous work by [Applied Science], he uses an acrylic rod as the rocket body and as the fuel. Bring a flame into the acrylic, apply oxygen from a canister at the other end of the body and voilà! The rocket engine starts nicely, and even better, the intensity of the burn can be controlled via the amount of oxygen provided.
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Retrotechtacular: The Golden Book Of Chemistry Experiments

November 11, 2016 by 33 Comments

Back in “the old days” (that is, when I was a kid), kids led lives of danger and excitement. We rode bikes with no protective gear. We stayed out roaming the streets after dark without adult supervision. We had toy guns that looked like real ones. Dentists gave us mercury to play with. We also blew things up and did other dangerous science experiments.

If you want a taste of what that was like, you might enjoy The Golden Book of Chemistry Experiments. The book, first published in 1960, offers to show you how to set up a home laboratory and provides 200 experiments. The colorfully illustrated book shows you how to do some basic lab work as well as offering some science history and terminology.

Want to make oxygen? There’s several methods on page 27. Page 28 covers making hydrogen. To test the hydrogen for purity, the suggest you collect a test tube full, invert it, and stick a match up to the tube. If the hydrogen is pure it will burn with a pop noise. If air is mixed it, it will explode. Yeah, that sound safe to us.

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Chemical Hacking At A Store Near You

November 11, 2016 by 56 Comments

Imagine for a minute that you aren’t an electronic-savvy Hackaday reader. But you find an old chemistry book at a garage sale and start reading it. It has lots of interesting looking experiments, but they all require chemicals with strange exotic names. One of them is ferric chloride. You could go find a scientific supply company, but that’s expensive and often difficult to deal with as an individual (for example, 2.5 liters of nitric acid costs over $300 for a case of six at a common lab supply company). Where would you go?

As an astute electronics guy (or gal) you probably know that ferric chloride is common for PCB etching, so you would check the electronic store down the street or maybe Radio Shack if you are lucky enough to find one that still stocks it.

So sometimes knowing where to look for a chemical is a key part of acquiring it, especially when the names are not the same. For example, do you have any amylose? No? That’s corn starch. Want to try making your own cadmium sulfide light sensor? Go to the art supply store and ask for cadmium yellow pigment. Need magnesium carbonate? Stop by a sporting goods store and ask for athlete’s chalk.

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