A plywood box with a clear plastic front is shown. Three needle gauges are visible on the front of the box, as well as a digital display, several switches, and some indicator lights. At the right of the box, a short copper tube extends from the box.

Building An X-Ray Crystallography Machine

July 7, 2025 by Aaron Beckendorf 10 Comments

X-ray crystallography, like mass spectroscopy and nuclear spectroscopy, is an extremely useful material characterization technique that is unfortunately hard for amateurs to perform. The physical operation isn’t too complicated, however, and as [Farben-X] shows, it’s entirely possible to build an X-ray diffractometer if you’re willing to deal with high voltages, ancient X-ray tubes, and soft X-rays.

[Farben-X] based his diffractometer around an old Soviet BSV-29 structural analysis X-ray tube, which emits X-rays through four beryllium windows. Two ZVS drivers power the tube: one to drive the electron gun’s filament, and one to feed a flyback transformer and Cockroft-Walton voltage multiplier which generate a potential across the tube. The most important part of the imaging system is the X-ray collimator, which [Farben-X] made out of a lead disk with a copper tube mounted in it. A 3D printer nozzle screws into each end of the tube, creating a very narrow path for X-rays, and thus a thin, mostly collimated beam.

To get good diffraction patterns from a crystal, it needed to be a single crystal, and to actually let the X-ray beam pass through, it needed to be a thin crystal. For this, [Farben-X] selected a sodium chloride crystal, a menthol crystal, and a thin sheet of mica. To grow large salt crystals, he used solvent vapor diffusion, which slowly dissolves a suitable solvent vapor in a salt solution, which decreases the salt’s solubility, leading to very slow, fine crystal growth. Afterwards, he redissolved portions of the resulting crystal to make it thinner.

The diffraction pattern generated by a sodium chloride crystal. A slide is shown with a dark black dot in the middle, surrounded by fainter dots. — The diffraction pattern generated by a sodium chloride crystal.

For the actual experiment, [Farben-X] passed the X-ray beam through the crystals, then recorded the diffraction patterns formed on a slide of X-ray sensitive film. This created a pattern of dots around the central beam, indicating diffracted beams. The mathematics for reverse-engineering the crystal structure from this is rather complicated, and [Farben-X] hadn’t gotten to it yet, but it should be possible.

We would recommend a great deal of caution to anyone considering replicating this – a few clips of X-rays inducing flashes in the camera sensor made us particularly concerned – but we do have to admire any hack that coaxed such impressive results out of such a rudimentary setup. If you’re interested in further reading, we’ve covered the basics of X-ray crystallography before. We’ve also seen a few X-ray machines.

Off-World Cement Tested For The First Time

September 30, 2019 by Tom Nardi 54 Comments

If the current Administration of the United States has their way, humans will return to the surface of the Moon far sooner than many had expected. But even if NASA can’t meet the aggressive timeline they’ve been given by the White House, it seems inevitable that there will be fresh boot prints on the lunar surface within the coming decades. Between commercial operators and international competition, we’re seeing the dawn of a New Space Race, with the ultimate goal being the long-term habitation of our nearest celestial neighbor.

Schmitt's dusty suit while retrieving samples from the Moon — An Apollo astronaut covered in lunar dust

But even with modern technology, it won’t be easy, and it certainly won’t be cheap. While commercial companies such as SpaceX have significantly reduced the cost of delivering payloads to the Moon, we’ll still need every advantage to ensure the economical viability of a lunar outpost. One approach is in situ resource utilization, where instead of transporting everything from Earth, locally sourced materials are used wherever possible. This technique would not only be useful on the Moon, but many believe it will be absolutely necessary if we’re to have any chance of sending a human mission to Mars.

One of the most interesting applications of this concept is the creation of a building material from the lunar regolith. Roughly analogous to soil here on Earth, regolith is a powdery substance made up of grains of rock and micrometeoroid fragments, and contains silicon, calcium, and iron. Mixed with water, or in some proposals sulfur, it’s believed the resulting concrete-like material could be used in much the same way it is here on Earth. Building dwellings in-place with this “lunarcrete” would be faster, cheaper, and easier than building a comparable structure on Earth and transporting it to the lunar surface.

Now, thanks to recent research performed aboard the International Space Station, we have a much better idea of what to expect when those first batches of locally-sourced concrete are mixed up on the Moon or Mars. Of course, like most things related to spaceflight, the reality has proved to be a bit more complex than expected.

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New Shape-Shifting Polymer Works Hard, Plays Hard

February 16, 2016 by Kristina Panos 22 Comments

A research group at the University of Rochester has developed a new polymer with some amazing traits. It can be stretched or manipulated into new shapes, and it will hold that shape until heat is applied. Shape-shifting polymers like this already exist, but this one is special: it can go back to its original shape when triggered by the heat of a human body. Oh, and it can also lift objects up to 1000 times its mass.

The group’s leader, chemical engineering professor [Mitch Anthamatten], is excited by the possibilities of this creation. When the material is stretched, strain is induced which deforms the chains and triggers crystallization. This crystallization is what makes it retain the new shape. Once heat is applied, the crystals are broken and the polymer returns to its original shape. These properties imply several biomedical applications like sutures and artificial skin. It could also be used for tailored-fit clothing or wearable technology.

The shape-shifting process creates elastic energy in the polymer, which means that it can do work while it springs back to normal. Careful application of molecular linkers made it possible for the group to dial in the so-called melting point at which the crystallization begins to break down. [Anthamatten] explains the special attributes of the material in one of the videos after the break. Another video shows examples of some of the work-related applications for the polymer—a stretched out strand can pull a toy truck up an incline or crush a dried seed pod.

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