Electron Microscopes Are Awesome: Everything You Didn’t Know You Wanted To Know

February 18, 2019 by 15 Comments

Electron microscopes were once the turf of research laboratories that could foot the hefty bill of procuring and maintaining such equipment. But old models have been finding their way into the hands of eager individuals who are giving us an inside look at the rare equipment. Before you start scouring Craigslist, go on a crash course of what you need to know with Adam McComb’s Hacker’s Guide to Electron Microscopy. He presented the talk at the 2018 Hackaday Superconference and the recording was just published, you’ll find it below.

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Reviving An Electron Microscope With Arduino

April 7, 2018 by 20 Comments

We don’t know about you, but when our friends ask us if we want to help them fix something, they’re usually talking about their computer, phone, or car. So far it’s never been about helping them rebuild an old electron microscope. But that’s exactly the request [Benjamin Blundell] got when a friend from a local hackerspace asked if he could take a look at a vintage Cambridge Stereoscan 200 they had found abandoned in a shed. Clearly we’re hanging out with the wrong group of people.

As you might imagine, the microscope was in desperate need of some love after spending time in considerably less than ideal conditions. While some of the hackerspace members started tackling the hardware side of the machine, [Benjamin] was tasked with finding a way to recover the contents of the scope’s ROM. While he’s still working on verification, the dumps he’s made so far of the various ROMs living inside the Stereoscan 200 have been promising and he believes he’s on the right track.

The microscope uses a mix of Texas Instruments 25L32 and 2516 chips, which [Benjamin] had to carefully pry out after making sure to document everything so he knew what went where. A few of the chips weren’t keen on being pulled from their home of 30-odd years, so there were a few broken pins, but on the whole the operation was a success.

Each chip was placed in a breadboard and wired up to an Arduino Mega, as it has enough digital pins to connect without needing a shift register. With the wiring fairly straightforward, [Benjamin] just needed to write up some code to read the contents of the chip, which he has graciously provided anyone else who might be working on a similar project. At this point he hasn’t found anything identifiable in his ROM dumps to prove that they’ve been made successfully, all he really knows right now is that he has something. At least it’s a start.

More and more of these older electron microscopes are getting a second lease on life thanks to dedicated hackers in their home labs. Makes you wonder if there’s ever going to be a piece of hardware the hacker community won’t bend to their will.

Scanning Electron Microscope Adds To Already Impressive Garage Lab

June 11, 2017 by 11 Comments

When you’re a high schooler who built a semiconductor fab in your garage, what’s next on your agenda? Why, adding a scanning electron microscope to your lab, naturally. How silly of you to ask.

When last we stumbled across the goings on in the most interesting garage in New Jersey, [Sam Zeloof] was giving a tour of his DIY semiconductor fabrication lab and showing off some of the devices he’s made there, including diodes and MOSFETs. As impressive as those components are, it’s the equipment he’s accumulated that really takes our breath away. So adding an eBay SEM to the mix only seems a natural progression, and a good reason to use some of the high vacuum gear he has. The video below shows [Sam] giving a tour of the 1990s-vintage instrument and shows images of various copper-sputtered samples, including a tick, which is apparently the state bird of New Jersey.

SEM hacks are by no means common around here, but they’re not unheard of. [Ben Krasnow] has used his to image cutting tools and phonograph records in action, and there are a few homebrew SEMs kicking around too. But our hats are off to [Sam] for yet another acquisition and a great tutorial to boot.

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Nascent Project: Open Source Scanning Electron Microscope

December 2, 2016 by 17 Comments

I used to have access to some pretty nice Scanning Electron Microscopes (a SEM) at my day job. While they are a bit more complex than a 3D printer, they are awfully handy when you need them. [Adam Guilmet] acquired a scrapped unit and started trying to figure out how to breathe life into it. His realization was that a SEM isn’t all that complicated by today’s standards. So he has set out to take what he has learned and build one from scrap.

In all fairness, he has a long way to go and is looking for help. He currently says, “[T]his is being powered by fairy dust, unicorn farts, and a budget that would make the poorest of students look like Donald Trump.” Still, he’s collected a lot of interesting data and we hope he can build a team that can succeed.

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Scanning Electron Microscope Images And Animations Pulled By Impressive Teensy LC Setup

September 5, 2015 by 29 Comments

When you’ve got a scanning electron microscope sitting around, you’re going to find ways to push the awesome envelope. [Ben Krasnow] is upping his SEM game with a new rig to improve image capture (video link) and more easily create animated GIFs and videos.

The color scheme of the SEM housing gives away its 80s vintage, and the height of image capture technology back then was a Polaroid camera mounted over the instrument’s CRT. No other video output was provided, so [Ben] dug into the blueprints and probed around till he found the high-resolution slow scan signal.

To make his Teensy-LC happy, he used a few op-amps to condition the analog signal for the greatest resolution and split out the digital sync signals, which he fed into the analog and digital ports respectively. [Ben] then goes into a great deal of useful detail on how he got the video data encoded and sent over USB for frame capture and GIF generation. Reading the ADC quickly without jitter and balancing data collection with transmission were tricky, but he has established a rock-solid system for it.

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Phonographs Through The Eye Of An Electron Microscope

June 16, 2015 by 32 Comments

Hackaday Prize judge [Ben Krasnow] has been busy lately. He’s put his scanning electron microscope (SEM) to work creating an animation of a phonograph needle playing a record. (YouTube link) This is the same 80’s SEM [Ben] hacked back in November. Unfortunately, [Ben’s]  JSM-T200 isn’t quite large enough to hold an entire 12″ LP, so he had to cut a small section of a record out. The vinyl mods weren’t done there though. SEMs need a conductive surface for imagingphono_anim_1. Vinyl is an insulator. [Ben] dealt with this by using his vacuum chamber to evaporate a thin layer of silver on the vinyl.

Just imaging the record wouldn’t be enough; [Ben] wanted an animation of a needle traveling through the record grove. He tore apart an old phonograph needle and installed it in on a copper wire in the SEM. Thanks to the dual stage setup of the JSM-T200, [Ben] was able to move the record-chip and needle independently. He could then move the record underneath the needle as if it were actually playing. [Ben] used his oscilloscope to record 60 frames, each spaced 50 microns apart. He used octave to process the data, and wound up with the awesome GIF animation you see on the left. 

pits[Ben] wasn’t done though. He checked out a few other recording formats, including CD and DVD optical media, and capacitance electronic disc, an obscure format from RCA which failed miserably in the market. The toughest challenge [Ben] faced was imaging the CD media. The familiar pits of a CD are stored on a thin aluminum layer sandwiched between the lacquer label and the plastic disc. He tried dissolving the plastic with chemicals, but enough plastic was left behind to distort the image. The solution turned out to be double-sided tape. Sticking some tape down on the CD and peeling it off cleanly removed the aluminum, and provided a sturdy substrate with which to mount the sample in the SEM.

We’re curious if stereo audio data can be extracted from the SEM images.  [Oona] managed to do this with a mono recording from a toy robot.  Who’s going to be the first one to break out the image analysis software and capture some audio from [Ben’s] images?

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A Scanning Electron Microscope For The Living Room

January 6, 2015 by 23 Comments

There are hackers who have soldering setups on the dining room table, and then there are hackers who have scanning electron microscopes in their living room. [Macona] is part of the latter group, with a Hitachi S-450 SEM he’s repaired and modified himself. [Macona] has documented the whole thing on Hackaday.io. The Hitachi came to him and a friend as a derelict. First it was broken, then stored for 10 years. It turned out the problem was a high voltage cable cut and spliced with electrical tape. The tape eventually broke down and shorted out the 500V supply. Thankfully the rectifier diodes were the only parts that needed to be replaced.

analog1The SEM sprang to life and gave [Macona] and a friend their first images. However, SEMs are finicky beasts. Eventually the filament burned out and needed to be replaced. New filaments are $500 US for a box of 10, which is more than [Macona] wanted to spend. It turns out filaments can be built at home. A bit of .089mm tungsten wire and a spot welder were all it took to fix the issue. Next to go bad was the scan amplifier. While SEMs use many exotic parts, the Hitachi used relatively common Sanyo STK070 audio amplifiers for the purpose – an easy fix!

One thing that makes this SEM unique is the is Energy Dispersive X-Ray Spectroscopy (EDX) unit attached to it. The fragile liquid nitrogen cooled sensor was working, but the 1980’s era signal processing computer was a bit too old to bring up. A friend and fellow SEM hobbiest gave [Macona] a slightly newer Kevex Sigma Gold signal processor, which was nearly a plug and play upgrade for his machine. The new processor processor also gave him digital beam controls and a digital output which could be used to capture images with a PC.

Once all the connections were made, the EDX worked surprisingly well, even finding gold in a uranium ore sample placed in the microscope.

Now that old scanning electron microscopes being retired, it’s only a matter of time before more us get a chance to join the ranks of [Jeri Ellsworth], [Ben Krasnow] and [Macona] with our own personal SEMs!