Nascent Project: Open Source Scanning Electron Microscope

December 2, 2016 by 17 Comments

I used to have access to some pretty nice Scanning Electron Microscopes (a SEM) at my day job. While they are a bit more complex than a 3D printer, they are awfully handy when you need them. [Adam Guilmet] acquired a scrapped unit and started trying to figure out how to breathe life into it. His realization was that a SEM isn’t all that complicated by today’s standards. So he has set out to take what he has learned and build one from scrap.

In all fairness, he has a long way to go and is looking for help. He currently says, “[T]his is being powered by fairy dust, unicorn farts, and a budget that would make the poorest of students look like Donald Trump.” Still, he’s collected a lot of interesting data and we hope he can build a team that can succeed.

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Scanning Electron Microscope Images And Animations Pulled By Impressive Teensy LC Setup

September 5, 2015 by 29 Comments

When you’ve got a scanning electron microscope sitting around, you’re going to find ways to push the awesome envelope. [Ben Krasnow] is upping his SEM game with a new rig to improve image capture (video link) and more easily create animated GIFs and videos.

The color scheme of the SEM housing gives away its 80s vintage, and the height of image capture technology back then was a Polaroid camera mounted over the instrument’s CRT. No other video output was provided, so [Ben] dug into the blueprints and probed around till he found the high-resolution slow scan signal.

To make his Teensy-LC happy, he used a few op-amps to condition the analog signal for the greatest resolution and split out the digital sync signals, which he fed into the analog and digital ports respectively. [Ben] then goes into a great deal of useful detail on how he got the video data encoded and sent over USB for frame capture and GIF generation. Reading the ADC quickly without jitter and balancing data collection with transmission were tricky, but he has established a rock-solid system for it.

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Phonographs Through The Eye Of An Electron Microscope

June 16, 2015 by 32 Comments

Hackaday Prize judge [Ben Krasnow] has been busy lately. He’s put his scanning electron microscope (SEM) to work creating an animation of a phonograph needle playing a record. (YouTube link) This is the same 80’s SEM [Ben] hacked back in November. Unfortunately, [Ben’s]  JSM-T200 isn’t quite large enough to hold an entire 12″ LP, so he had to cut a small section of a record out. The vinyl mods weren’t done there though. SEMs need a conductive surface for imagingphono_anim_1. Vinyl is an insulator. [Ben] dealt with this by using his vacuum chamber to evaporate a thin layer of silver on the vinyl.

Just imaging the record wouldn’t be enough; [Ben] wanted an animation of a needle traveling through the record grove. He tore apart an old phonograph needle and installed it in on a copper wire in the SEM. Thanks to the dual stage setup of the JSM-T200, [Ben] was able to move the record-chip and needle independently. He could then move the record underneath the needle as if it were actually playing. [Ben] used his oscilloscope to record 60 frames, each spaced 50 microns apart. He used octave to process the data, and wound up with the awesome GIF animation you see on the left. 

pits[Ben] wasn’t done though. He checked out a few other recording formats, including CD and DVD optical media, and capacitance electronic disc, an obscure format from RCA which failed miserably in the market. The toughest challenge [Ben] faced was imaging the CD media. The familiar pits of a CD are stored on a thin aluminum layer sandwiched between the lacquer label and the plastic disc. He tried dissolving the plastic with chemicals, but enough plastic was left behind to distort the image. The solution turned out to be double-sided tape. Sticking some tape down on the CD and peeling it off cleanly removed the aluminum, and provided a sturdy substrate with which to mount the sample in the SEM.

We’re curious if stereo audio data can be extracted from the SEM images.  [Oona] managed to do this with a mono recording from a toy robot.  Who’s going to be the first one to break out the image analysis software and capture some audio from [Ben’s] images?

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A Scanning Electron Microscope For The Living Room

January 6, 2015 by 23 Comments

There are hackers who have soldering setups on the dining room table, and then there are hackers who have scanning electron microscopes in their living room. [Macona] is part of the latter group, with a Hitachi S-450 SEM he’s repaired and modified himself. [Macona] has documented the whole thing on Hackaday.io. The Hitachi came to him and a friend as a derelict. First it was broken, then stored for 10 years. It turned out the problem was a high voltage cable cut and spliced with electrical tape. The tape eventually broke down and shorted out the 500V supply. Thankfully the rectifier diodes were the only parts that needed to be replaced.

analog1The SEM sprang to life and gave [Macona] and a friend their first images. However, SEMs are finicky beasts. Eventually the filament burned out and needed to be replaced. New filaments are $500 US for a box of 10, which is more than [Macona] wanted to spend. It turns out filaments can be built at home. A bit of .089mm tungsten wire and a spot welder were all it took to fix the issue. Next to go bad was the scan amplifier. While SEMs use many exotic parts, the Hitachi used relatively common Sanyo STK070 audio amplifiers for the purpose – an easy fix!

One thing that makes this SEM unique is the is Energy Dispersive X-Ray Spectroscopy (EDX) unit attached to it. The fragile liquid nitrogen cooled sensor was working, but the 1980’s era signal processing computer was a bit too old to bring up. A friend and fellow SEM hobbiest gave [Macona] a slightly newer Kevex Sigma Gold signal processor, which was nearly a plug and play upgrade for his machine. The new processor processor also gave him digital beam controls and a digital output which could be used to capture images with a PC.

Once all the connections were made, the EDX worked surprisingly well, even finding gold in a uranium ore sample placed in the microscope.

Now that old scanning electron microscopes being retired, it’s only a matter of time before more us get a chance to join the ranks of [Jeri Ellsworth], [Ben Krasnow] and [Macona] with our own personal SEMs!

[Ben Krasnow] Hacks A Scanning Electron Microscope

September 3, 2014 by 32 Comments

[Ben Krasnow] is quite possibly the only hacker with a Scanning Electron Microscope (SEM) collection. He’s acquired a JEOL JSM-T200, which was hot stuff back in the early 1980’s. [Ben] got a great deal, too.  He only had to pay shipping from Sweden to his garage. The SEM was actually dropped during shipment, but thankfully the only damage was a loose CRT neck plug. The JSM-T200 joins [Ben’s] homemade SEM, his DIY CT scanner, the perfect cookie machine, and a host of other projects in his lab.

The JSM-T200 is old tech; the primary way to store an image from this machine is through a screen-mounted Polaroid camera, much like an old oscilloscope. However, it still has a lot in common with current SEMs. In live video modes, an SEM can only collect one or two reflected electrons off a given section of a target. This creates a low contrast ghostly image we’ve come to associate with SEMs.

Attempting to fire more electrons at the target will de-focus the beam due to the electrons repelling each other. Trying to fire the electrons from higher voltages will just embed them into the target. Even SEMs with newer technology have to contend with these issues. Luckily, there is a way around them.

When “writing to photo”, the microscope switches to a slow scan mode, where the image is scanned over a period of a minute. This slower scan gives the microscope extra time to fire and collect more electrons – leading to a much better image. Using this mode, [Ben] discovered his microscope was capable of producing high-resolution digital images. It just needed a digital acquisition subsystem grafted on.

Click past the break to see how [Ben] modernized his microscope!

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Electron Beam Control In A Scanning Electron Microscope

April 13, 2014 by 6 Comments

Electron

A few years ago [Ben Krasnow] built a scanning electron microscope from a few parts he had sitting around. He’s done a few overviews of how he built his SEM, but now he’s put up a great video on how to control electrons, focus them into a point, and scan a sample.

The basic idea behind a scanning electron microscope is to shoot electrons down a tube, focus them into a point, and scan a conductive sample and detect the secondary electrons shot off the sample and display them on an oscilloscope. [Ben] is generating electrons with a small tungsten filament at the top of his electron ‘stack’. Being like charged, these electrons naturally fan out, so a good bit of electron optics are required to get a small point.

Focusing is done through a series of pinholes and electrostatic deflectors, much like you’d see in an old oscilloscope CRT. In the video, you can see [Ben] shooting electrons and displaying a Christmas tree graphic  onto a piece of phosphor-coated glass. He has a pretty big scanning area in his SEM, more than enough to look at a few chips, wafers, and whatever other crazy stuff is coming out of [Ben]’s lab.

Video below, along with the three-year-old overview of the entire microscope.

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DIY Scanning Electron Microscope

March 23, 2011 by 22 Comments

[Ben Krasnow]  has recently completed a home-built scanning electron microscope and has posted a video of it in action on his blog.

The build itself was done quite creatively using many off-the shelf components. We particularly like how long threaded brass rods were used not only for the supports, but also to maintain column alignment and fine-tune the spacing between the various beam focusing components.  A large glass “bell jar” covers the entire apparatus and is sealed to the bottom plate when the air is removed from within by a mechanical vacuum pump.

In order to produce an image, an electron gun similar to one found in a conventional CRT television tube accelerates the electrons with a 5kV potential from the top of the microscope downwards through a long copper column. Along the way the beam is focused and manipulated by electronic lenses in much the same way that light would be handled by conventional optical lenses. Near the base of the main column there are electrostatic deflection plates placed orthogonally in the X and Y directions that allow for precise scanning of the beam across the sample’s surface. When this high-energy electron beam is scanned across the sample, scattering surface electrons are then picked up by a nearby detector consisting of a phosphor screen and photomultiplier – a system that supposedly allows for higher sensitivity than trying to measure the small numbers of electrons directly.

Although the resolution of the first few scans is only around 50uM, this early success clearly shows that the device functions as intended and will provide a great starting point for future refinement with the final goal being resolutions down to the 1uM range.

Despite Ben’s reassurance that the x-rays produced at this energy level  won’t even penetrate the glass chamber, you can be sure that if we ever visit his garage we will definitely be donning some tin foil protection like these guys.

[Thanks kyle]

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