reduction

11 Articles

Desert Island Acetylene From Seashells And Driftwood

November 15, 2024 by 35 Comments

[MacGyver] would be proud of [Hyperspace Pirate]’s rough and ready method of producing acetylene gas from seashells and driftwood.

Acetylene, made by decomposing calcium carbide with water, is a vitally important industrial gas. Not only as a precursor in many chemical processes, but also as the fuel for the famous “blue wrench,” a tool without which auto mechanics working in the Rust Belt would be reduced to tears. To avoid this, [Hyperspace Pirate] started by beachcombing for the raw materials: shells to make calcium oxide and wood to make charcoal. Charcoal is pretty easy; you just cook chunks of wood in a reducing environment to drive off everything but the carbon. Making calcium oxide from the calcium carbonate in the shells isn’t much harder, with ground seashells heated in a propane-fired furnace to release carbon dioxide.

With the raw ingredients in hand, things get a little tricky. Making calcium carbide requires a lot of heat, far more than a simple propane burner can provide. [Hyperspace Pirate] decided to go with an electric arc furnace, to which end he cannibalized a 120 V to 240 V step-up converter for its toroidal transformer, which with a few extra windings provided the needed current to run an arc through carbon electrodes. This generated the needed heat, and then some, as the ceramic firebrick he was using to contain the inferno melted. After rewinding the melted secondary windings on his makeshift transformer and switching to a stainless steel crucible, he was able to make enough calcium carbide to generate an impressive amount of acetylene. The video below documents the process and the sooty results, as well as details a little of the excitement that metal acetylides offer.

For more about acetylene and its many uses, [This Old Tony] has you covered.

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Gears Are Old And Busted, Capstans Are Cool

June 3, 2024 by 44 Comments

Zero backlash, high “gear” reduction, high torque transparency, silent operation, and low cost. What is this miracle speed reduction technology, you ask? Well, it’s shoelaces and a bunch of 3D printed plastic, at least in [Aaed Musa]’s latest installment in his series on developing his own robot dog.

OK, the shoelaces were only used in the first proof of concept. [Aaed] shortly upgrades to steel cable, and finds out that steel fatigues and snaps after a few hours. He settles on Dyneema DM-20, a flexible yet non-stretching synthetic rope.

Before it’s all over, he got a five-bar linkage plotting with a pencil on the table and a quadriped leg jumping up and down on the table — to failure. All in all, it points to a great future, and we can’t wait to see the dog-bot that’s going to come out of this.

There’s nothing secret about using capstan drives, but we often wonder why we don’t see cable-powered robotics used more in the hacker world. [Aaed] makes the case that it pairs better with 3D printing than gears, where the surface irregularities really bind. If you want to get a jumpstart, the test fixture that he’s using is available on GitHub.

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Mining And Refining: Titanium, Our Youngest Industrial Metal

December 5, 2023 by 9 Comments

Earlier in this series, we made the case for copper being “the metal that built technology.” Some readers took issue with that statement, noting correctly that meteoric iron and gold were worked long before our ancestors were able to locate and exploit natural copper outcroppings, therefore beating copper to the historical punch. That seems to miss the point, though; figuring out how to fashion gold decorations and iron trinkets doesn’t seem like building the foundations for industry. Learning to make tools from copper, either pure or alloyed with tin to make bronze? Now that’s how you build an industrial base.

So now comes the time for us to make the case for our most recent addition to humanity’s stable of industrial metals: titanium. Despite having been discovered in 1791, titanium remained locked away inside abundantly distributed ores until the 1940s, when the technological demands of a World War coupled with a growing chemical prowess and command of sufficient energy allowed us to finally wrest the “element of the gods” from its minerals. The suddenness of it all is breathtaking, too; in 1945, titanium was still a fantastically expensive laboratory oddity, but just a decade later, we were producing it by the (still very expensive) ton and building an entirely new aerospace industry around the metal.

In this installment of “Mining and Refining,” we’ll take a look at titanium and see why it took us over 11,000 years to figure out how to put it to work for us.

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Copper Be Gone: The Chemistry Behind PCB Etching

August 31, 2023 by 33 Comments

For a lot of reasons, home etching of PCBs is somewhat of a dying art. The main reason is the rise of quick-turn PCB fabrication services, of course; when you can send your Gerbers off and receive back a box with a dozen or so professionally made PCBs for a couple of bucks, why would you want to mess with etching your own?

Convenience and cost aside, there are a ton of valid reasons to spin up your own boards, ranging from not having to wait for shipping to just wanting to control the process yourself. Whichever camp you’re in, though, it pays to know what’s going on when your plain copper-clad board, adorned with your precious artwork, slips into the etching tank and becomes a printed circuit board. What exactly is going on in there to remove the copper? And how does the etching method affect the final product? Let’s take a look at a few of the more popular etching methods to understand the chemistry behind your boards.

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Harmonic Drive Uses Compliant Mechanism To Slim Down

April 7, 2021 by 15 Comments

[Levi Janssen] has a secret: he doesn’t like harmonic drives. But rather than abandon the torque-amplifying transmission completely, he decided to see about improving them using 3D-printed compliant mechanisms.

For the uninitiated, harmonic drives, also known as strain-wave gears, are a compact, high-torque gearbox that has become popular with “robotic dog” makers and other roboticists. The idea is to have a rigid, internally-toothed outer ring nested around an externally-toothed, flexible cup. A wave generator rotates within the inside cup, stretching it so that it meshes with the outer ring. The two gears differ by only a couple of teeth, meaning that very high gear ratios can be achieved, which makes them great for the joints of robot legs.

[Levi]’s problem with the harmonic drive is that due to the depth of the flexible spline cup, compactness is not among its virtues. His idea is to couple the flex spline to the output of the drive through a flat spring, one that allows flexion as the wave generator rotates but transmits torque efficiently. The entire prototype is 3D-printed, except for the wave generator bearings and stepper motor, and put to the test.

As the video below shows after the excellent introduction to harmonic drives, the concept works, but it’s not without its limitations. Even lightly loaded, the drive made some unpleasant crunching sounds as the PLA springs gave out. We could easily see that being replaced with, say, a steel spring, either machined or cut on a water-jet machine. That might solve the most obvious problem and make [Levi]’s dream of a compact harmonic drive a reality. Of course, we have seen pretty compact strain-wave gears before.

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Simple Demo Shows The Potential Of Magnetic Gears

April 13, 2020 by 27 Comments

We’ve probably all used gears in our projects at one time or another, and even if we’re not familiar with the engineering details, the principles of transmitting torque through meshed teeth are pretty easy to understand. Magnetic gears, though, are a little less intuitive, which is why we appreciated stumbling upon this magnetic gear drivetrain demonstration project.

[William Fraser]’s demo may be simple, but it’s a great introduction to magnetic gearing. The stator is a block of wood with twelve bolts to act as pole pieces, closely spaced in a circle around a shaft. Both ends of the shaft have rotors, one with eleven pairs of neodymium magnets arranged in a circle with alternating polarity, and a pinion on the other side of the stator with a single pair of magnets. When the pinion is spun, the magnetic flux across the pole pieces forces the rotor to revolve in the opposite direction at a 12:1 ratio.

Watching the video below, it would be easy to assume such an arrangement would only work for low torque applications, but [William] demonstrated that the system could take a significant load before clutching out. That could even be a feature for some applications. We’ve got an “Ask Hackaday” article on magnetic gears if you want to dive a little deeper and see what these interesting mechanisms are good for.

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Cheap PSoC Enables Electrochemistry Research

August 4, 2018 by 8 Comments

You may think electrochemistry sounds like an esoteric field where lab-coated scientists labor away over sophisticated instruments and publish papers that only other electrochemists could love. And you’d be right, but only partially, because electrochemistry touches almost everything in modern life. For proof of that look no further than your nearest pocket, assuming that’s where you keep your smartphone and the electrochemical cell that powers it.

Electrochemistry is the study of the electrical properties of chemical reactions and does indeed need sophisticated instrumentation. That doesn’t mean the instruments have to break the grant budget, though, as [Kyle Lopin] shows with this dead-simple potentiostat built with one chip and one capacitor. A potentiostat controls the voltage on an electrode in an electrochemical cell. Such cells have three electrodes — a working electrode, a reference electrode, and a counter electrode. The flow of electrons between these electrodes and through the solutions under study reveal important properties about the reduction and oxidation states of the reaction. Rather than connect his cell to an expensive potentiostat, [Kyle] used a Cypress programmable system-on-chip development board to do everything. All that’s needed is to plug the PSoC into a USB port for programming, connect the electrodes to GPIO pins, and optionally add a 100 nF capacitor to improve the onboard DAC’s accuracy. The video below covers the whole process, albeit with a barely audible voiceover.

Still not sure about electrochemistry? Check out this 2018 Hackaday Prize entry that uses the electrochemistry of life to bring cell phones back to life.

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