glass

64 Articles

Stresses Revealed With A Polariscope

April 1, 2022 by 13 Comments

There are a lot of ways that stresses can show up, at least when discussing materials science. Cracks in concrete are a common enough example, but any catastrophic failure in a material is often attributable to some stress that couldn’t be withstood. If you’re interested in viewing those stresses before they result in damage to the underlying material, take a look at this DIY polariscope which can view internal stresses in glass and other clear objects.

The polariscope takes its name from the fact that it uses polarized light to view the internal structure of a transparent object such as glass. When the polarized light passes through glass in a certain way, the stresses show up as lighter areas thanks to the stressed glass bending the light back into view. This one is constructed with a polarizing filter placed in front of an LCD screen set to display a completely white image. When glass is placed between the screen and the filter no light is seen through the polariscope unless there are stresses in the glass. Even placing a force on an otherwise un-stressed glass tube can show this effect, and [Advanced Tinkering], this project’s creator, has several other creations which show this effect in striking detail.

The effect can also be observed as colored areas in other plastic materials as well. It’s an interesting tool which can help anyone who frequently works with glass, but it’s also interesting on its own to see clues left behind from the manufacturing process of various household items. We’ve seen some other investigative methods for determining how other household items are mass produced as well, like this project which breaks down the injection molding process.

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Glassblowing For The Lab

March 4, 2022 by 20 Comments

There was a time when ordering some glassware from a distributor meant making a sizable minimum order, sending a check in the mail and waiting weeks for a box full of — hopefully intact — glassware to arrive. In those days, blowing your own glassware from glass tubes was fairly common and [Wheeler Scientific] has been doing a series on just how to do that. Even if you aren’t interested in building a chemistry lab, you might find the latest episode on making a gas discharge tube worth a watch. There are several videos and you can see a few of them below.

Of course, blowing glass is literally playing with fire, so be careful. Most important rule? Don’t inhale. Then again, for a lot of things, blowing glass doesn’t involve you actually blowing, but it is more like bending and shaping and — technically — what he shows is lampwork, not actual glassblowing, but that’s a technicality.

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Tech In Plain Sight: Primitive Engineering Materials

December 22, 2021 by 33 Comments

It isn’t an uncommon science fiction trope for our hero to be in a situation where there is no technology. Maybe she’s back in the past or on a faraway planet. The Professor from Gilligan’s Island comes to mind, too. I’d bet the average Hacakday reader could do pretty well in that kind of situation, but there’s one thing that’s often overlooked: materials. Sure, you can build a radio. But can you make wire? Or metal plates for a capacitor? Or a speaker? We tend to overlook how many abstractions we use when we build. Even turning trees into lumber isn’t a totally obvious process.

People are by their very nature always looking for ways to use the things around them. Even 300,000 years ago, people would find rocks and use them as tools. It wasn’t long before they found that some rocks could shape other rocks to form useful shapes like axes. But the age of engineered materials is much younger. Whether clay, metal, glass, or more obviously plastics, these materials are significantly more useful than rocks tied to sticks, but making them in the first place is an engineering story all on its own.

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Everything You Always Wanted To Know About Radioactive Lenses

August 7, 2021 by 45 Comments

We think of radioactive material as something buried away in bunkers with bombs, power plants, and maybe some exotic medical equipment. But turns out, there are little bits of radiation in the water, our soil, bananas, granite countertops, smoke detectors, and even some camera lenses. Camera lenses? A few decades ago, camera companies added rare elements like thorium to their glass to change the optical properties in desirable ways. The downside? Well, it made the lenses somewhat radioactive.  A post by [lenslegend] explains it all.

Exotic elements such as Thorium, Lanthanum and Zirconium are added to glass mixtures to create the high refractive indexes necessary in sophisticated lens designs. Selection of premium quantities of glass from the large glass pots, stringent spectrophotometric tests after stress and strain checks provide the valuable raw glass for ultimate use in lens elements.
—Konica Hexanon Lens Guide, Konica Camera Company, 1972

According to [lenslegend] the practice started in 1945 with Kodak. However, by the 1980s, consumer distaste for radioactive things and concern for factory workers ended the production of hot camera lenses.

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Tiny Tesla Valves Etched In Glass

June 20, 2021 by 8 Comments

While it’s in vogue right now to name fancy new technology after Tesla, the actual inventor had plenty of his own creations that would come to bear his namesake, including Tesla coils, Tesla oscillators, Tesla turbines and even the infamous Tesla tower. One of the lesser known inventions of his is the Tesla valve, a check valve that allows flow in one direction without any moving parts, and [Huygens Optics] shows us a method of etching tiny versions of these valves into glass.

The build starts out with a fairly lengthy warning, which is standard practice when working with hydroflouric acid. The acid is needed to actually perform the etching, but it’s much more complicated than a typical etch due to the small size of the Tesla valves. He starts by mixing a buffered oxide etch, a mix of the hydroflouric acid, ammonia, and hydrochloric acid, which gives a much more even etching than any single acid alone. Similar to etching PCBs, a protective mask is needed to ensure that the etch only occurs where it’s needed. For that there are several options, each with their own benefits and downsides, but in the end [Huygens Optics] ends up with one of the smallest Tesla valves ever produced.

In fact, the valves are so small that they can only be seen with the aid of a microscope. While viewing them under the microscope he was able to test with a small drop of water to confirm that they do work as intended. And, while the valves that he is creating in this build are designed to work on liquids, [Huygens Optics] notes that the reason for making them this small was to make tiny optical components which they are known for.

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Injection-Molded Glass Breakthrough Shatters Ceiling Of Work Methods

June 10, 2021 by 36 Comments

Glass is one of humanity’s oldest materials, and it is still used widely for everything from drinking vessels and packaging to optics and communications. Unfortunately, the methods for working with glass are stuck in the past. Most methods require a lot of high heat in the range of 1500 °C to 2000 °C, and they’re all limited in the complexity of shapes that can be made.

As far as making shapes goes, glass can be blown and molten glass pressed into molds. Glass can also be ground, etched, or cast in a kiln. Glass would be fantastic for many applications if it weren’t for the whole limited geometry thing. Because of the limitations of forming glass, some optic lenses are made with polymers, even though glass has better optical characteristics.

Ideally, glass could be injection molded like plastic. The benefits of this would be twofold: more intricate shapes would be possible, and they would have a much faster manufacturing time. Well, the wait is over. Researchers at Germany’s University of Freiburg have figured out a way to apply injection molding to glass. And it’s not just any glass — they’ve made highly-quality, transparent fused quartz glass, and they did it at lower temperatures than traditional methods. The team used x-ray diffraction to verify that the glass is amorphous and free of crystals, and were able to confirm its optical transparency three ways — light microscopy, UV-visible, and infrared measurements. All it revealed was a tiny bit of dust, which is to be expected outside of a clean room.

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Micromachining Glass With A Laser — Very, Very Slowly

January 9, 2021 by 28 Comments

When it comes to machining, the material that springs to mind is likely to be aluminum, steel, or plastic. We don’t necessarily think of glass as a material suitable for machining, at least not in the chuck-it-up-in-the-lathe sense. But glass is a material that needs to be shaped, too, and there are a bunch of different ways to accomplish that. Few, though, are as interesting as micromachining glass with laser-induced plasma bubbles. (Video, embedded below.)

The video below is from [Zachary Tong]. It runs a bit on the longish side, but we found it just chock full of information. The process, formally known as “laser-induced backside wet-etching,” uses a laser to blast away at a tank of copper sulfate. When a piece of glass is suspended on the surface of the solution and the laser is focused through the glass from the top, some interesting things happen.

The first pulse of the laser vaporizes the solution and decomposes the copper sulfate. Copper adsorbs onto the glass surface inside the protective vapor bubble, which lasts long enough for a second laser pulse to come along. That pulse heats up the adsorbed copper and the vapor in the original bubble, enough to melt a tiny bit of the glass. As the process is repeated, small features are slowly etched into the underside of the glass. [Zachary] demonstrates all this in the video, as well as what can go wrong when the settings are a bit off. There’s also some great high-speed footage of the process that’s worth the price of admission alone.

We doubt this process will be a mainstream method anytime soon, not least because it requires a 50-Watt Nd:YAG fiber laser. But it’s an interesting process that reminds us of [Zachary]’s other laser explorations, like using a laser and Kapton to make graphene supercapacitors.

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