Automated Rig Grows Big, Beautiful Crystals Fast

December 12, 2024 by Dan Maloney 8 Comments

We haven’t seen [Les Wright] in a while, and with the release of his new video, we know why — he’s been busy growing crystals.

Now, that might seem confusing to anyone who has done the classic “Crystal Garden” trick with table salt and laundry bluing, or tried to get a bit of rock candy out of a supersaturated sugar solution. Sure, growing crystals takes time, but it’s not exactly hard work. But [Les] isn’t in the market for any old crystals. Rather, he needs super-sized, optically clear crystals of potassium dihydrogen phosphate, or KDP, which are useful as frequency doublers for lasers. [Les] has detailed his need for KDP crystals before and even grown some nice ones, but he wanted to step up his game and grow some real whoppers.

And boy, did he ever. Fair warning; the video below is long and has a lot of detail on crystal-growing theory, but it’s well worth it for anyone taking the plunge. [Les] ended up building an automated crystal lab, housing it in an old server enclosure for temperature and dust control. The crystals are grown on a custom-built armature that slowly rotates in a supersaturated solution of KDP which is carefully transitioned through a specific temperature profile under Arduino control. As a bonus, he programmed the rig to take photographs of the growing crystals at intervals; the resulting time-lapse sequences are as gorgeous as the crystals, one of which grew to 40 grams in only a week.

We’re keen to see how [Les] puts these crystals to work, and to learn exactly what a “Pockels Cell” is and why you’d want one. In the meantime, if you’re interested in how the crystals that make the whole world work are made, check out our deep dive into silicon.

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VNAs And Crystals

December 6, 2024 by Al Williams 7 Comments

Oscillators may use crystals as precise tuned circuits. If you have a vector network analyzer (VNA) — or even some basic test equipment — you can use it to learn the parameters of a crystal. [All Electronics Channel] has the details, and you can see how in the video below.

There was a time when a VNA was an exotic piece of gear, but these days they are relatively common. Crystal parameters are important because crystals have a series resonance and a parallel resonance and they are not at the same frequency. You also may need to know how much loading capacitance you have to supply to get the crystal at the right frequency.

Sometimes, you want to pull the crystal frequency, and the parameters will help you figure that out, too. It can also help if you have a crystal specified as series in a parallel-mode oscillator or vice versa.

If you don’t have a VNA, you can use a tracking signal generator, as [Grégory] shows towards the middle of the video. The quality of a tuned circuit depends on the Q factor, and crystals have a very high Q factor.

We did something similar in 2018. The other way to pull a crystal frequency is a bit extreme.

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Cat-o-Matic 3000 Serves Your Feline Masters

December 1, 2023 by Kristina Panos 8 Comments

When you have three cats and three humans, you have one problem: feeding them on a schedule without over or under feeding them. Even if there was only one human in the equation, the Cat-o-Matic 3000 would still be a useful tool.

Essentially, it’s a traffic light for cats — where green means you are go for feeding, and red means the cat was just fed. Yellow, of course, means the cat is either half-full or half-empty, depending on your outlook.

The brains of this operation is an ATmega88PA leftover from another project. There’s a no-name voltage regulator that steps up the two AA cells to 5 volts. Timing comes from a 32 kHz crystal that allows the microcontroller to stay in power-saving sleep mode for long periods of time.

Creator [0xCAFEAFFE] says the firmware was cobbled together from other projects. Essentially, it wakes up once per second to increment the uptime counter and then goes back to sleep. Short-pressing a button shows the feeding status, and long-pressing it will reset the timer.

Wanna make a cat status indicator without electronics? Give flexures a try.

Growing Simple Crystals For Non-Linear Optics Experiments

July 6, 2023 by Dan Maloney 18 Comments

Here’s an exercise for you: type “crystals” into your favorite search engine and see what you get. If you’re anything like us, you’ll get a bunch of pseudoscientific posts about the healing power of crystals, along with offers to buy the same at exorbitant prices. But woo-woo aside, certain crystals do have seemingly magical powers — like the ability to turn light from one color into another.

None of this is magic, of course. Rather, as optics aficionado [Les Wright] explains, non-linear optics is all about physics. Big physics, too, like the kind that made the National Ignition Facility the first fusion research outfit to reach the “break-even” point, at least in terms of optical energy. To do so, they need to convert megajoules of infrared laser beams all the way across the visible spectrum into the ultraviolet, relying on huge crystals of deuterated potassium dihydrogen phosphate (KDP) to do so. Depending on how they’re cut, crystals of these sorts have non-linear optical properties like second-harmonic generation, which combines two input photons into a single output photon with twice the energy of the original. This results in a halving of the wavelength of the input, which doubles the frequency.

While the process used at the NIF produces crystals of enormous proportions, [Les] has more modest needs and thus a simpler process. His KDP is an off-the-shelf chemical, nothing fancy about it, which is added to boiling water to make a saturated solution. A little of the solution is poured out into a watch glass to make seed crystals, and everything is allowed to cool slowly. A nice seed crystal is glued to a piece of monofilament fishing line and suspended in the saturated solution, and with enough time a good-sized crystal forms. Placed into the beam path of a 1,064 nm IR laser and rotated carefully relative to the beam, the crystal easily produces a brilliant green laser output.

This is fascinating stuff, and we’re looking forward to seeing where [Les] goes with this. Polishing the crystals to make them optically cleaner would be a good next step, as would perhaps growing even larger crystals.

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Building A Receiver With The ProgRock2 Programmable Crystal

April 28, 2023 by Lewin Day 11 Comments

Crystals are key to a lot of radio designs. They act as a stable frequency source and ensure you’re listening to (or transmitting on) exactly the right bit of the radio spectrum. [Q26] decided to use the ProgRock2 “programmable crystal” to build a receiver that could tune multiple frequencies without the usual traditional tuning circuitry.

The ProgRock2 is designed as a tiny PCB that can be dropped into a circuit to replace a traditional crystal. The oscillators onboard are programmable from 3.5KHz to 200 MHz, and can be GPS discliplined for accuracy. It’s programmable over a micro USB pot, and can be set to output 24 different frequencies, in eight banks of three. When a bank is selected, the three frequencies will be output on the Clock0, Clock1, and Clock2 pins.There was some confusion regarding the bank selection on the ProgRock2. It’s done by binary, with eight banks selected by grounding the BANK0, BANK1, and BANK2 pins. For example, grounding BANK2 and BANK0 would activate bank 5 (as 101 in binary equals 5). Once this was figured out, [Q26] was on top of things.

In his design, [Q26] hooked up the ProgRock2 into his receiver in place of the regular crystal. Frequency selection is performed by flipping three switches to select banks 0 to 7. It’s an easy way to flip between different frequencies accurately, and is of particular use for situations where you might only listen on a limited selection of amateur channels.

For precision use, we can definitely see the value of a “programmable crystal” oscillator like this. We’ve looked at the fate of some major crystal manufacturers before, too. Video after the break.

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How To Grow Your Own Pyramid Salt Crystals

October 13, 2022 by Lewin Day 22 Comments

The regular granular table salt you’re used to isn’t the most attractive-looking seasoning out there, even given its fundamentally compelling flavor. You don’t have to settle for boring old salt anymore though, because [Chase] has shown us you can grow your own pyramid salt crystals at home!

Pyramid salt crystals can grow naturally, and typically occur in locations where salt pools are undisturbed under the warmth of the sun. However, it’s possible to grow them on purpose, too. As a bonus, their hollow structure means they dissolve very quickly on the tongue, and can taste “saltier” than typical granular salt.

To grow your own, you’ll need a bag of salt, which is mixed with some water. You’ll want to do so in a glass dish, as the salty solution you’ll be making can ruin metal cookware. The dish can then be heated up on an electric hotplate, which is used to heat the solution to between 60 and 70°C.

A small amount of food-grade potassium alum is also added to the solution to calm the convection currents in the heated solution, allowing the crystals to form gently without sticking and clumping together. As the water boils away, the rectangular-pyramidal crystals grow.

Naturally, you must be careful before eating the results of any home-grown lab experiments. However, [Chase] reports having licked some of the crystals and has confirmed they do indeed taste salty. [Chase] also notes several ways in which the parameters can be changed to grow different types of pyramid crystals, too.

We’ve featured [Chase]’s crystal-growing work before. If you’ve got your own cool DIY crystal projects cooking up in the lab, be sure to let us know!

Multiband Crystal Radio Set Pulls Out All The Stops

April 28, 2022 by Dan Maloney 23 Comments

Most crystal radio receivers have a decidedly “field expedient” look to them. Fashioned as they often are from a few turns of wire around an oatmeal container and a safety pin scratching the surface of a razor blade, the whole assembly often does a great impersonation of a pile of trash whose appearance gives little hope of actually working. And yet work they do, usually, pulling radio signals out of thin air as if by magic.

Not all crystal sets take this slapdash approach, of course, and some, like this homebrew multiband crystal receiver, aim for a feature set and fit and finish that goes way beyond the norm. The “Husky” crystal set, as it’s called by its creator [alvenh], looks like it fell through a time warp right from the 1920s. The electronics are based on the Australian “Mystery Set” circuit, with modifications to make the receiver tunable over multiple bands. Rather than the traditional galena crystal and cat’s whisker detector, a pair of1N34A germanium diodes are used as rectifiers — one for demodulating the audio signal, and the other to drive a microammeter to indicate signal strength. A cat’s whisker is included for looks, though, mounted to the black acrylic front panel along with nice chunky knobs and homebrew rotary switches for band selection and antenna.

As nice as the details on the electronics are, it’s the case that really sells this build. Using quarter-sawn oak salvaged from old floorboards. The joinery is beautiful and the hardware is period correct; we especially appreciate the work that went into transforming a common flat washer into a nickel-plated escutcheon for the lock — because every radio needs a lock.

Congratulations to [Alvenh] for pulling off such a wonderful build, and really celebrating the craftsmanship of the early days of radio. Need some crystal radio theory before tackling your build? Check out [Greg Charvat]’s crystal radio deep dive.