Sketch of the UED setup at EPFL, 1) Electron gun, 2) High-Voltage connector, 3) Photo-cathode, 4) Anode, 5) Collimating solenoid, 6) Steering plates, 7) Focusing solenoid, 8) RF cavity, 9) Sample holder, 10) Cryostat, 11) Electron detector, 12) Turbo pump, 13) Ion gauge. Credit: Proceedings of the National Academy of Sciences (2024). DOI: 10.1073/pnas.2316438121

Using Femtosecond Laser Pulses To Induce Metastable Hidden States In Magnetite

July 20, 2024 by Maya Posch No comments

Hidden states are a fascinating aspect of matter, as these can not normally be reached via natural processes (i.e. non-ergodic), but we can establish them using laser photoexcitation. Although these hidden states are generally very unstable and will often decay within a nanosecond, there is evidence for more persistent states in e.g. vanadates. As for practical uses of these states, electronics and related fields are often mentioned. This is also the focus in the press release by the Ecole Polytechnique Federale de Lausanne (EPFL) when reporting on establishing hidden states in magnetite (Fe₃O₄), with the study published in PNAS (Arxiv preprint link).

[B. Truc] and colleagues used two laser frequencies to either make the magnetite more conductive (800 nm) or a better insulator (400 nm). The transition takes on the order of 50 picoseconds, allowing for fairly rapid switching between these metastable states. Naturally, turning this into practical applications will require a lot more work, especially considering the need for femtosecond pulsed lasers to control the process, which makes it significantly more cumbersome than semiconductor technology. Its main use at this point in time will remain a fascinating demonstration of these hidden states of matter.

Making Music By Probing Magnetite Crystals

May 9, 2023 by Dave Rowntree 2 Comments

Well, noises anyway. [Dmitry Morozov] and [Alexandra Gavrilova] present an interesting electronics-based art installation, which probes a large chunk of crystalline magnetite, using a pair of servo-mounted probes, ‘measuring’ the surface conductivity and generating some sound and visuals.

It appears to have only one degree of freedom per probe, so we’re not so sure all that much of the surface gets probed per run, but however it works it produces some interesting, almost random results. The premise is that the point-to-point surface resistivity is unpredictable due to the chaotically formed crystals all jumbled up, but somehow uses these measured data to generate some waveshapes vaguely reminiscent of the resistivity profile of the sample, the output of which is then fed into a sound synthesis application and pumped out of a speaker. It certainly looks fun.

From a constructional perspective, hardware is based around a LattePanda fed samples by an ADS1115 ADC, which presumably is also responsible for driving the LCD monitor and the sound system. An Arduino is also wedged in there perhaps for servo-driving duty, maybe also as part of the signal chain from the probes, but that is just a guess on our part. The software uses the VVVV (Visual Live-programming suite) and the Pure Data environment.

We haven’t seen magnetite used for this type of application before, we tend to see it as a source of Iron for DIY knifemaking, as a medium to help separate DNA or just to make nanoparticles, for erm, reasons.

This Stainless Steel Knife Build Starts With Raw Iron Ore

August 6, 2022 by Dan Maloney 11 Comments

Making knives at home has become a popular hobby, thanks partly to reality TV and the free time and idle hands afforded by lockdowns. Depending on how far you get into the hobby, builds can range from assembling and finishing a kit with pre-forged parts, to actual blacksmithing with a hammer and anvil. But pretty much every build includes steel from a commercial supplier.

Not this one. Rather than buy his metal from the usual sources, [Thoisoi]’s first stop was an iron mine in the Italian Alps, where he picked up a chunk of iron ore — magnetite, to be precise. Smelting one’s own iron from raw ore and alloying it into steel is generally not a backyard project thanks to the high temperatures needed, a problem [Thoisoi] solved with the magic of thermite. The iron oxide and aluminum in the thermite mix react in an exceptionally exothermic manner to generate elemental iron, which under controlled conditions can be captured as a more or less pure ingot, ready for forging.

After a test with commercially obtained iron oxide, [Thoisoi] tried his pulverized magnetite. And thanks to the addition of goodies like graphite, manganese, nickel, silicon, and chromium, he was eventually able to create a sizable lump of 402 stainless steel. He turned the metal over to an actual blacksmith for rough forging; it sure seemed to act like steel on the anvil. The finished knife looks good and performs well, and the blade has the characteristic look of stainless. Not a bad result, and all at the cost of a couple of clay flowerpots.

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DIY Furnace Smelts Magnetite Sand Into An Impressive Chef’s Knife

March 9, 2021 by Mike Szczys 24 Comments

Some people order their raw materials from a factory, missing out on 99% of the fun… or suffering, we’re not sure which. To make that call, you need to look in on the process [IllyriaD] used to collect magnetite sand and turn it into a wicked-looking chef’s knife.

This began by collecting 150 pounds (!) of magnetic dirt from dry lake beds while hiking using a magnet pickup tool with release lever that he got from Harbor Freight. Several repeated magnetic refining passes separated the black ore from non-metallic sands ready for the furnace that he built. That is used to fire up the raw materials using 150 pounds of charcoal, changing the chemical composition by adding carbon and resulting in a gnarly lump of iron known as a bloom.

From there, it’s just a matter of beating the iron bloom into submission over at the anvil. [IllyriaD] details the process of flattening it out to a bar shape, then folding it over. Seven total folds are made for 128 layers, and in the gallery there’s a fantastic image that captures the striation when viewed on end. After being sharpened and polished, you can see where the bevel descends through those layers.

It’s delightful to see people working through the old ways and proving you don’t need a factory, as long as your true goal is to explore the process itself. Does this leave you wanting even more? [IllyriaD] left some insight about the process in the comments of the reddit thread. You probably also want to check out the tile-roofed hut built by [PrimitiveTechnology] without any modern tools.

Digging In The Dirt Yields Homebrew Inductors

September 13, 2020 by Dan Maloney 16 Comments

Let’s say you’re stranded on a desert island and want to get the news from the outside world. You’ll have to build your own crystal radio, of course, but your parts bin is nowhere to be found and Digi-Key isn’t delivering. So you’ll need to MacGuyver some components. Capacitors are easy with a couple of pieces of tinfoil, and a rectifier can be made from a pencil and a razor blade. But what about an inductor? Sure, air-core inductors will work, but just because you’re marooned doesn’t mean you’ve abandoned your engineering principles. Luckily, you’ve read [AC7ZL]’s treatise of making inductors from dirt, and with sand in abundance, you’re able to harvest enough material to put together some passable ferrite-core inductors.

Obviously, making your own inductive elements isn’t practical even in fanciful and contrived situations, but that doesn’t make the doing of it any less cool. The story begins with a walk in the Arizona desert many years ago, where [AC7ZL], aka [H.P. Friedrichs], spied bands of dark sand shooting through the underlying lighter sediments. These bands turned out to be magnetite, one of many iron-bearing minerals found in the area. Using a powerful magnet from an old hard drive and a plastic food container, he was able to harvest magnetite sand in abundance and refine it with multiple washing steps.

After experimentally determining the material’s permeability — about 2.3 H/m — [AC7ZL] proceeded with some practical applications. He was able to make a bar antenna for an AM radio by packing the sand into a PVC pipe and rewinding the coils around it. More permanent cores were made by mixing the sand with polyester resin and casting it into bars. Toroids were machined from fat bars of the composite on a lathe, much to the detriment of the cutting tools used.

The full-length PDF account of [AC7ZL]’s experiments makes for fascinating reading — the inductive elements he was able to create all performed great in everything from a Joule Thief to a Hartley oscillator up to 27 MHz. We love these kinds of stories, which remind us of some of the work being done by [Simplifier] and others.

Cheap And Easy Magnetic DNA Separation Method Needs Your Help

August 28, 2017 by Dan Maloney 5 Comments

When you consider that almost every single cell in your body has more than a meter of DNA coiled up inside its nucleus, it seems like it should be pretty easy to get some to study. But with all the other cellular gunk in a crude preparation, DNA can be quite hard to isolate. That’s where this cheap and easy magnetic DNA separation method comes in. If it can be optimized and tested with some help from the citizen science community.

Commercial DNA separation methods generally involve mixing silica beads into crude cell fractions; the DNA preferentially binds to the silica, making it possible to mechanically separate it from the rest of the cellular junk. But rather than using a centrifuge to isolate the DNA, [Justin] from The Thought Emporium figured that magnets might do a better job. It’s not a new idea — biotech companies offer magnetic separation beads commercially, but at too steep a price for [Justin]’s budget. His hack comes from making magnetite particles from common iron compounds like PCB etchant and moss killer, and household ammonia cleaner. The magnetite particles are then coated with sodium silicate solution, also known as waterglass. The silica coating should allow the beads to bind to DNA, with the magnetic core taking care of separation.

[Justin] was in the process of testing his method when he lost access to the needed instruments, so he’s appealing to the larger science community for help optimizing his technique. Based on his track record of success in fields ranging from satellite tracking to graphene production, we’ll bet he’ll nail this one too.

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Make Your Own Magnetic Ink

July 17, 2012 by Mike Szczys 12 Comments

Here [Catarina Mota] is showing off a ring of magnetic ink printed on a piece of paper. It’s strong enough to hold a disc magnet in place when the paper is raised vertically. This strength comes from mixing your own batch of ink.

Magnetic ink has been around a long time and is most often used in banking. The account number and routing number on the bottom left of paper checks are printed in magnetic ink to allow for automated recognition. Iron oxide is charged by the reader as it passes through. In this case, magnetite is used as the doping agent as it has very strong ferromagnetic properties. By mixing it with acrylic medium in a vortex mixer you end up with a homogeneous ink.

There’s a quick demo after the break that shows how well this printed ring holds the magnet. What are some things for which you would use this ink? Leave a comment to let us know.

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