There’s no debating that metallic sodium is exciting stuff, but getting your hands on some can be problematic, what with the need to ship it in a mineral oil bath to keep it from exploding. So why not make your own? No problem, just pass a few thousand amps of current through an 800° pot of molten table salt. Easy as pie.
Thankfully, there’s now a more approachable method courtesy of this clever chemical hack that makes metallic sodium in quantity without using electrolysis. [NurdRage], aka [Dr. N. Butyl Lithium], has developed a process to extract metallic sodium from sodium hydroxide. In fact, everything [NurdRage] used to make the large slugs of sodium is easily and cheaply available – NaOH from drain cleaner, magnesium from fire starters, and mineral oil to keep things calm. The reaction requires an unusual catalyst – menthol – which is easily obtained online. He also gave the reaction a jump-start with a small amount of sodium metal, which can be produced by the lower-yielding but far more spectacular thermochemical dioxane method; lithium harvested from old batteries can be substituted in a pinch. The reaction will require a great deal of care to make sure nothing goes wrong, but in the end, sizable chunks of the soft, gray metal are produced at phenomenal yields of 90% and more. The video below walks you through the whole process.
It looks as though [NurdRage]’s method can be scaled up substantially or done in repeated small batches to create even more sodium. But what do you do when you make too much sodium metal and need to dispose of it? Not a problem.
Continue reading “Common Chemicals Combine To Make Metallic Sodium”
On the face of it, PCB production seems to pretty much have been reduced to practice. Hobbyists have been etching their own boards forever, and the custom PCB fabrication market is rich with vendors whose capabilities span the gamut from dead simple one-side through-hole boards to the finest pitch multilayer SMD boards imaginable.
So why on Earth would we need yet another way to make PCBs? Because as [Ben Krasnow] points out, the ability to turn almost any plastic surface into a PCB can be really handy, and is not necessarily something the fab houses handle right now. The video below shows how [Ben] came up with his method, which went down a non-obvious path that was part chemistry experiment, part materials science. The basic idea is to use electroless copper plating, a method of depositing copper onto a substrate without using electrolysis.
This allows non-conductive substrates — [Ben] used small parts printed with a Formlabs SLA printer — to be plated with enough copper to form solderable traces. The chemistry involved in this is not trivial; there are catalysts and surfactants and saturated solutions of copper sulfate to manage. And even once he dialed that in, he had to figure out how to make traces and vias with a laser cutter. It was eventually successful, but it took a lot of work. Check out the video below to see how he got there, and where he plans to go next.
You’ve got to hand it to [Ben]; when he decides to explore something, he goes all in. We appreciate his dedication, whether he’s using candles to explore magnetohydrodynamics or making plasma with a high-speed jet of water.
Continue reading “Chemistry and Lasers Turn Any Plastic Surface Into a PCB”
[Ben Krasnow] has an inimitable knack for choosing the most interesting concepts for his experiments. We’re sure it’s a combination of base knowledge and epic-curiosity. This time around he’s showing off a vintage cigarette lighter whose quirk is not needing to be “struck” to produce a flame. It’s a catalytic lighter that uses platinum to ignite methanol vapors.
The concept shown in the video below is platinum’s catalyst properties with some types of flammable gasses. The image above shows the cap of the lighter which includes a protective cage around a hunk of fine platinum powder known as platinum black. It is suspended by platinum wire and as the hydrogen passes by the reaction causes the platinum black and wire to glow red-hot.
This simple, quick experiment fills in our own knowledge gaps. We were already familiar with the role that catalytic converters play in automobiles; consuming any unburned hydrocarbons before they exit a vehicle’s exhaust system. We also know the these devices are targets for thieves seeking the platinum (and other metals like palladium and rhodium) found inside. Now we know exactly how catalytic converters work and the integral role that platinum plays in the process. All thanks to [Ben’s] demonstration of how this lighter works.
Now, if you wear a platinum wedding band and your hand passes a jet of hydrogen are you likely to get burned?
Continue reading “The Platinum Catalyst Use in a Vintage Lighter”