gold

19 Articles

The green CRT display of a scanning-electron microscope is shown, displaying small particles.

DIY Calibration Target For Electron Microscopes

June 12, 2025 by 3 Comments

It’s a problem that few of us will ever face, but if you ever have to calibrate your scanning electron microscope, you’ll need a resolution target with a high contrast under an electron beam. This requires an extremely small pattern of alternating high and low-density materials, which [ProjectsInFlight] created in his latest video by depositing gold nanoparticles on a silicon slide.

[ProjectsInFlight]’s scanning electron microscope came from a lab that discarded it as nonfunctional, and as we’ve seen before, he’s since been getting it back into working condition. When it was new, it could magnify 200,000 times and resolve features of 5.5 nm, and a resolution target with a range of feature sizes would indicate how high a magnification the microscope could still reach. [ProjectsInFlight] could also use the target to make before-and-after comparisons for his repairs, and to properly adjust the electron beam.

Since it’s easy to get very flat silicon wafers, [ProjectsInFlight] settled on these as the low-density portion of the target, and deposited a range of sizes of gold nanoparticles onto them as the high-density portion. To make the nanoparticles, he started by dissolving a small sample of gold in aqua regia to make chloroauric acid, then reduced this back to gold nanoparticles using sodium citrate. This gave particles in the 50-100 nanometer range, but [ProjectsInFlight] also needed some larger particles. This proved troublesome for a while, until he learned that he needed to cool the reaction temperature solution to near freezing before making the nanoparticles.

Using these particles, [ProjectsInFlight] was able to tune the astigmatism settings on the microscope’s electron beam so that it could clearly resolve the larger particles, and just barely see the smaller particles – quite an achievement considering that they’re under 100 nanometers across!

Electron microscopes are still a pretty rare build, but not unheard-of. If you ever find one that’s broken, it could be a worthwhile investment.

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Hackaday Links: May 4, 2025

May 4, 2025 by 14 Comments

By now, you’ve probably heard about Kosmos 482, a Soviet probe destined for Venus in 1972 that fell a bit short of the mark and stayed in Earth orbit for the last 53 years. Soon enough, though, the lander will make its fiery return; exactly where and when remain a mystery, but it should be sometime in the coming week. We talked about the return of Kosmos briefly on this week’s podcast and even joked a bit about how cool it would be if the parachute that would have been used for the descent to Venus had somehow deployed over its half-century in space. We might have been onto something, as astrophotographer Ralf Vanderburgh has taken some pictures of the spacecraft that seem to show a structure connected to and trailing behind it. The chute is probably in pretty bad shape after 50 years of UV torture, but how cool is that?

Parachute or not, chances are good that the 495-kilogram spacecraft, built to not only land on Venus but to survive the heat, pressure, and corrosive effects of the hellish planet’s atmosphere, will at least partially survive reentry into Earth’s more welcoming environs. That’s a good news, bad news thing: good news that we might be able to recover a priceless artifact of late-Cold War space technology, bad news to anyone on the surface near where this thing lands. If Kosmos 482 does manage to do some damage, it won’t be the first time. Shortly after launch, pieces of titanium rained down on New Zealand after the probe’s booster failed to send it on its way to Venus, damaging crops and starting some fires. The Soviets, ever secretive about their space exploits until they could claim complete success, disavowed the debris and denied responsibility for it. That made the farmers whose fields they fell in the rightful owners, which is also pretty cool. We doubt that the long-lost Kosmos lander will get the same treatment, but it would be nice if it did.

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Flashlight shining through gold leaf on glass

Shining Through: Germanium And Gold Leaf Transparency

January 5, 2025 by 26 Comments

Germanium. It might sound like just another periodic table entry (number 32, to be exact), but in the world of infrared light, it’s anything but ordinary. A recent video by [The Action Lab] dives into the fascinating property of germanium being transparent to infrared light. This might sound like sci-fi jargon, but it’s a real phenomenon that can be easily demonstrated with nothing more than a flashlight and a germanium coin. If you want to see how that looks, watch the video on how it’s done.

The fun doesn’t stop at germanium. In experiments, thin layers of gold—yes, the real deal—allowed visible light to shine through, provided the metal was reduced to a thickness of 100 nanometers (or: gold leaf). These hacks reveal something incredible: light interacts with materials in ways we don’t normally observe.

For instance, infrared light, with its lower energy, can pass through germanium, while visible light cannot. And while solid gold might seem impenetrable, its ultra-thin form becomes translucent, demonstrating the delicate dance of electromagnetic waves and electrons.

The implications of these discoveries aren’t just academic. From infrared cameras to optics used in space exploration, understanding these interactions has unlocked breakthroughs in technology. Has this article inspired you to craft something new? Or have you explored an effect similar to this? Let us know in the comments!

We usually take our germanium in the form of a diode. Or, maybe, a transistor.

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Restoring A Vintage CGA Card With Homebrew HASL

June 12, 2024 by 26 Comments

Right off the bat, we’ll stipulate that what [Adrian] is doing in the video below isn’t actual hot air solder leveling. But we thought the results of his card-edge connector restoration on a CGA video card from the early 80s was pretty slick, and worth keeping in mind for other applications.

The back story is that [Adrian], of “Digital Basement” YouTube fame, came across an original IBM video card from the early days of the IBM-PC. The card was unceremoniously dumped, probably due to the badly corroded pins on the card-edge bus connector. The damage appeared to be related to a leaking battery — the corrosion had that sickly look that seems to only come from the guts of batteries — leading him to try cleaning the formerly gold-plated pins. He chose naval jelly rust remover for the job; for those unfamiliar with this product, it’s mostly phosphoric acid mixed with thickeners and is used as a rust remover.

The naval jelly certainly did the trick, but left the gold-plated pins a little worse for the wear. Getting them back to their previous state wasn’t on the table, but protecting them with a thin layer of solder was easy enough. [Adrian] used liquid rosin flux and a generous layer of 60:40 solder, which was followed by removing the excess with desoldering braid. That worked great and got the pins on both sides of the board into good shape.

[Adrian] also mentioned a friend who recommended using toilet paper to wick up excess solder, but sadly he didn’t demonstrate that method. Sounds a little sketchy, but maybe we’ll give it a try. As for making this more HASL-like, maybe heating up the excess solder with an iron and blasting the excess off with some compressed air would be worth a try.

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Nanotechnology In Ancient Rome? There Is Evidence

January 26, 2024 by 47 Comments

Anything related to nanotechnology feels fairly modern, doesn’t it? Although Richard Feynman planted the seeds of the idea in 1959, the word itself didn’t really get formed until the 70s or 80s, depending on who you ask. But there is evidence that nanotechnology could have existed as far back as the 4th century in ancient Rome.

That evidence lies in this, the Lycurgus cup. It’s an example of dichroic glass — that is, glass that takes on a different color depending on the light source. In this case, the opaque green of front lighting gives way to glowing red when light is shining through it. The mythology that explains the scene varies a bit, but the main character is King Lycurgus, king of Edoni in Thrace.

So how does it work? The glass contains extremely small quantities of colloidal gold and silver — nanoparticles of gold to produce the red, and silver particles to make the milky green. The composition of the Lycurgus cup was puzzling until the 1990s, when small pieces of the same type of glass were discovered in ancient Roman ruins and analyzed. The particles in the Lycurgus cup are thought to be the size of one thousandth of a grain of table salt — substantial enough to reflect light without blocking it.

The question is, how much did the Romans know about what they were doing? Did they really have the means to grind these particles into dust and purposely infuse them, or could this dichroic glass have been produced purely by accident? Be sure to check out the videos after the break that discuss this fascinating piece of drinkware.

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Making The One Ring By Electroplating Gold On A 3D Print

January 12, 2023 by 11 Comments

Electroplating is a great way to add strength or shine to a 3D print. However, we don’t see too many people trying it with gold. [HEN3DRIK] isn’t afraid to experiment, though, and pulled off some amazing, high-quality jewelry-grade plating!

The design for the project was the so-called Ring of Power from Lord of the Rings. The print was created on a resin printer at a high quality level, washed thoroughly to remove any remaining resin, and then cured. The print was then post-processed with sandpaper to make it as smooth as possible. Conductive paint was then applied, ready to take on the plating layers. [HEN3DRIK] first started by plating copper to build up a tough base layer, then nickel to prevent mixing between the copper and gold. The gold is then finally plated on top. Plating the copper is done with the ring constantly rotating to get as even a coat as possible. In contrast, the gold plating is done with a brush to avoid wasting the highly-expensive plating solution.

The final result is a gleaming gold ring that probably feels strangely light in the hand. The technique is time consuming, thanks to the need to plate multiple layers, but the results are to die for. We’ve seen [HEN3DRIK]’s fine work before, too. Video after the break.

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Scavenging CDs For Flexible Parts

August 1, 2022 by 42 Comments

CDs are becoming largely obsolete now, thanks to the speed of the internet and the reliability and low costs of other storage media. To help keep all of this plastic out of the landfills, many have been attempting to find uses for these old discs. One of the more intriguing methods of reprurposing CDs was recently published in Nature, which details a process to harvest and produce flexible biosensors from them.

The process involves exposing the CD to acetone for 90 seconds to loosen the material, then transferring the reflective layer to a plastic tape. From there, various cutting tools can be used to create the correct pattern for the substrate of the biosensor. This has been shown to be a much more cost-effective method to produce this type of material when compared to modern production methods, and can also be performed with readily available parts and supplies as well.

The only downside to this method is that it was only tested out on CDs which used gold as the conducting layer. The much more common aluminum discs were not tested, but it could be possible with some additional research. So, if you have a bunch of CD-Rs laying around, you’re going to need to find something else to do with those instead.

Thanks to [shinwachi] for the tip!